Lézerindukált plazmaspektrométer és ICP-tömegspektrométer alkalmazása kriminalisztikai vizsgálatokban
Copyright (c) 2024 Stadler Tamás, Zihné Perényi Katalin, Bozó Csaba, Molnár Andrea, Szoldán Zsolt, Vörös Tamás
This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.
Absztrakt
A korszerű elemanalitikai technikák alkalmazása a kriminalisztikai anyagvizsgálatban egyre hangsúlyosabb szerephez jut. A Nemzeti Szakértői és Kutató Központban 2021-ben üzembe helyezett lézerindukált plazmaspektrométerrel (LIBS) és induktív csatolású plazma-tömegspektrométerrel (ICP-MS) talajon, építőanyagon, üvegen, festéken, ragasztószalagon és biológiai anyagmaradványokon végzett vizsgálatok bizonyították a módszer használhatóságát az azonosító és összehasonlító vizsgálatokban. A nagy érzékenységű tömegspektrométeres nyomelem-analízis a korábban rendelkezésre álló módszereinkhez képest pontosabb vizsgálatot tesz lehetővé. A lézerablációs mintabevitellel az egyes mintarészletek, míg oldatos feltárással a teljes minta anyagának átlagos elemi (izotópos) összetétele mérhető. Tanulmányunkban bemutatjuk a LIBS- és ICP-MS-technikák működésének alapjait, valamint kriminalisztikai alkalmazásukat, az elmúlt években vizsgált eseteken keresztül.
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